HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178422083, compound → HCID 178422098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178422083 | HCID 178422083 | — |
| Reactant | HCID 178453727 | HCID 178453727 | — |
| Product | HCID 178422098 | HCID 178422098 | — |
Reaction Steps
The title compound was prepared according to the procedure described in the preparation of 2-((2S)-bicyclo[2.2.1]heptan-2-ylamino)-5-methyl-5-(piperidin-4-ylmethyl)thiazol-4(5H)-one by using tert-butyl 2-(3-(4-((2-((2S)-bicyclo[2.2.1]heptan-2-ylamino)-5-methyl-4-oxo-4,5-dihydrothiazol-5-yl)methyl)piperidine-1-carbonyl)phenoxy)ethylcarbamate (689 mg, 1.18 mmol) as the starting material. The title compound was obtained as an off-white solid (531 mg). MS (ESI, pos. ion) m/z: 485 (M+H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541592B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-afdc2e93269742faae0d9d2acafb0ea0 |
| Source note | uspto-grants-2013_09 |