HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-nitroaniline → 10,12-Dichlorodibenzo[a,c]phenazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-nitroaniline | HCID 75893 | — |
| Reactant | 1,2-Phenanthrenedione | HCID 3080566 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 10,12-Dichlorodibenzo[a,c]phenazine | HCID 21391728 | 81% |
Reaction Steps
When 0.12 mole each of 2,4-dichloro-6-nitroaniline and phenanthrenequinone were reacted by the method of Example 1, 24 g. (81 percent yield) of 10,12-dichlorodibenzo[a,c]phenazine, mp = 221°-222° C. (acetone), were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064127 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-cf5c608cf4994a89b522be502c1d94b8 |
| Source note | uspto-grants-1977_12 |