HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 5-(tert-Butyl)-3-chloro-4-hydroxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | 3-(tert-Butyl)-4-hydroxybenzaldehyde | HCID 3017618 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 5-(tert-Butyl)-3-chloro-4-hydroxybenzaldehyde | HCID 3017619 | — |
Reaction Steps
Chlorine gas was passed into a solution of 3-tert-butyl-4-hydroxybenzaldehyde (2.5 gm) in acetic acid (20 ml) for 1 hour. The solution was poured into water and the product collected. Recrystallisation from aqueous ethanol gave 3-tert-butyl-5-chloro-4-hydroxybenzaldehyde m.p. 123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064266 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-35231d5d4e214396a1b80ff85b230e62 |
| Source note | uspto-grants-1977_12 |