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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 463539Generated: October 23, 2026

2-Propanol, 1,3-dichloro-, 2-carbamate → 1,3-dichloropropan-2-yl carbamate;ditridecyl (Z)-but-2-enedioate

https://huagongshe.com/en/reaction/463539

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Propanol, 1,3-dichloro-, 2-carbamateHCID 68516—
Reactant1,1-Bis(tert-butylperoxy)cyclohexaneHCID 76359—
Reactant2-Butenedioic acid (2Z)-, 1,4-ditridecyl esterHCID 6437427—
Product1,3-dichloropropan-2-yl carbamate;ditridecyl (Z)-but-2-enedioateHCID 131712900—

Reaction Conditions

Temperature110 °C

Reaction Steps

To a 500 ml resin kettle equipped with an overhead stirrer and containing 200 g of Flo Mo 36 C (ethoxylated castor oil) were added 50 g ditridecyl maleate and 6 g 1,1-bis(t-butylperoxy)cyclohexane (available from Witco Chemical Company under the tradename USP-400P). The mixture was then heated to 110° C. for 4 hours under nitrogen to yield a viscous liquid surfactant of the invention (Surfactant No. 54).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04520140
Source datasetuspto-grants-1985_05
ORD IDord-3414ce7107c148798ef167c89ac2f26c
Source noteuspto-grants-1985_05