HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 46408Generated: October 26, 2026
Triphenylphosphine → (Ethoxymethyl)(triphenyl)phosphanium chloride
https://huagongshe.com/reaction/46408
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Chloromethyl ethyl ether | HCID 18523 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | (Ethoxymethyl)(triphenyl)phosphanium chloride | HCID 21470303 | — |
Reaction Steps
A solution of 99.66 g of triphenylphosphine and 37.82 g of chloromethyl ethyl ether in 240 ml of dry benzene was stirred and refluxed (84° C.) for 6 hours. The mixture then was chilled and filtered to give 7, as a white solid, mp 205°-206° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04173463 |
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| Source dataset | uspto-grants-1979_11 |
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| ORD ID | ord-3204c8b2736246ee820e2cf7f1906092 |
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| Source note | uspto-grants-1979_11 |
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