1,4-Cyclohexanedimethanol → Cyclohexanedimethanol

Reaction equation

[CH:1]1([CH2:9][OH:10])[CH2:6][CH2:5][CH:4](CO)[CH2:3][CH2:2]1.C1(=O)[O:17][CH2:16]CCCC1>>[C:1]1([CH2:9][OH:10])([CH2:16][OH:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

Participants

Reactant 2

HCID 77351,4-Cyclohexanedimethanol

HCID 10401epsilon-CAPROLACTONE

Product 1

HCID 250594Cyclohexanedimethanol

Procedure

Using a procedure similar to that for Experiment 1, various ratios of 1,4-cyclohexanedimethanol were reacted with ε-caprolactone. Table 1 gives the ratio of moles to viscosity and amount of unreacted cyclohexanedimethanol.

Sources & evidence

ORD record: ord-310e34c58e67481cbd0f283fed3fe0a0
Source dataset: uspto-grants-1992_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05159047

Reaction notes

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