HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octene → Gamma-Decalactone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octene | HCID 8125 | — |
| Reactant | Potassium Acetate | HCID 517044 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Gamma-Decalactone | HCID 12813 | 61% |
Reaction Steps
Octene-1 in an amount of 2.24 g. and 5.1 g. of Mn2O3 (comprising two equivalents of Mn+3 based on titration value) were refluxed under nitrogen in 200 ml. glacial acetic acid containing 60 g. potassium acetate. After a period of less than two hours, gamma-n-hexyl-butyrolactone was obtained in a yield of 61%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04175089 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-43204c96c25d493ba43892f30698f076 |
| Source note | uspto-grants-1979_11 |