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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 46753Generated: October 26, 2026

Benzaldehyde → Cyano(phenyl)methyl 2-methylpropanoate

https://huagongshe.com/reaction/46753

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzaldehydeHCID 240—
ReactantIsobutyric anhydrideHCID 7346—
ReactantSodium CyanideHCID 8929—
SolventWaterHCID 962—
ProductCyano(phenyl)methyl 2-methylpropanoateHCID 13536647—

Reaction Conditions

Temperature25 °C

Reaction Steps

A 100-ml round-bottomed flask equipped with a magnetic stirrer was charged with isobutyric anhydride (10 mmol), benzaldehyde (10 mmol), a mixture of alkanes (25 ml) having a boiling range of from 62° C. to 82° C., sodium cyanide (12 mmol) and water (3 ml). The mixture formed was stirred at a temperature of 25° C. The table presents the yields of the title ester after the reaction times indicated (Embodiment IV).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04175094
Source datasetuspto-grants-1979_11
ORD IDord-b8b0d7af08bb45c5b88e08b5a8efd0a7
Source noteuspto-grants-1979_11