3-Aminopicolinic acid → 3-Amino-N-(2-methoxyethyl)-N-methylpicolinamide

HRID 467735

Reaction equation

HRID 467735 reaction equation
[NH2:1][C:2]1[C:3]([C:8]([OH:10])=O)=[N:4][CH:5]=[CH:6][CH:7]=1.[CH3:11][O:12][CH2:13][CH2:14][NH:15][CH3:16]>>[NH2:1][C:2]1[C:3]([C:8]([N:15]([CH2:14][CH2:13][O:12][CH3:11])[CH3:16])=[O:10])=[N:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 738363-Aminopicolinic acidHCID 300977(2-Methoxyethyl)(methyl)amine

Product 1

HCID 700969433-Amino-N-(2-methoxyethyl)-N-methylpicolinamideYield 85%

Procedure

According to the procedure described in example 29, 3-aminopicolinic acid was reacted with 2-methoxy-N-methylethanamine to give the title compound (85%) as colourless viscous oil.

Sources & evidence

ORD record
ord-e2722df999c1485383d3111e2f5a26db
Source dataset
uspto-grants-2014_01
Patent number
US08623866B2

Linked notes

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