HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylaniline → N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylaniline | HCID 6894 | — |
| Reactant | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Product | N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline | HCID 13017553 | — |
Reaction Steps
2-methyl-3-chloroaniline (0.25 mole) and 4-chlorobenzaldehyde (0.25 mole) were ground in a mortar. The mixture was heated, with stirring in a water bath for 1.5 hours. Distillation at reduced pressure gave N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline as a second fraction; B.p. 139° C./0.020 mm.; m.p. 79°-81° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04176198 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-1954ed2e6b654a29afa1d9e4851e850b |
| Source note | uspto-grants-1979_11 |