1-Methylimidazole → HCID 178418501, compound

Reaction equation

[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[CH:3]1.[Cl:7][CH2:8][O:9][C:10](=[S:12])[CH3:11]>>[Cl-:7].[C:10]([O:9][CH2:8][N+:4]1[CH:5]=[CH:6][N:2]([CH3:1])[CH:3]=1)(=[S:12])[CH3:11]

Participants

Reactant 2

HCID 13901-Methylimidazole

HCID 53833355Chloromethylthioacetate

Product 1

HCID 178418501HCID 178418501, compound

Procedure

To 0.7 g (8.52 millimoles) of 1-methylimidazole was added slowly and with cooling, 1.5 g of (16.2 millimoles) chloromethylthioacetate. The solution solidified in 10 minutes and was left stoppered at room temperature overnight.

Workup

temperaturewith cooling
waitwas left
waitstoppered at room temperature overnight

Sources & evidence

ORD record: ord-a75e54f6a7504dcd907a03e3ff22457e
Source dataset: uspto-grants-1988_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04727151

Reaction notes

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