Myrtanal → 2,10-Epoxypinane

HRID 473392

Reaction equation

HRID 473392 reaction equation
[CH3:1][C:2]1([CH3:11])[CH:7]2[CH2:8][CH:3]1[CH2:4][CH2:5][CH:6]2[CH:9]=[O:10]>C(#N)C>[CH3:1][C:2]1([CH3:11])[CH:7]2[CH2:8][CH:3]1[CH2:4][CH2:5][C:6]12[O:10][CH2:9]1

Participants

3

Reactant 1

HCID 165266Myrtanal

Product 1

HCID 930462,10-Epoxypinane

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

Material I was used in the procedure described in example 11 in acetonitrile and it was observed that after 2 h of reaction time, the conversion was less than 23% and selectivity for myrtanal was 53%.

Workup

  1. customafter 2 h
  2. customof reaction time

Sources & evidence

ORD record
ord-d2b07a6ffe344dbc871b02080446543e
Source dataset
uspto-grants-2014_01
Patent number
US08633338B2

Linked notes

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