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Phosphoric Acid → HCID 178513043, compound

HRID 480520
Notes
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Reaction equation

HRID 480520 reaction equation
[C:1]([N:3]=[C:4]([NH2:6])[NH2:5])#[N:2].[P:7](=[O:11])([OH:10])([OH:9])[OH:8]>O>[P:7]([OH:11])([OH:10])([OH:9])=[O:8].[C:4]([NH:3][C:1]([NH2:2])=[O:8])(=[NH:6])[NH2:5]
ParticipantsProcedureSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 1004Phosphoric AcidHCID 10005Dicyandiamide

Product 1

HCID 178513043HCID 178513043, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

In a preferred method, Oberley '010 reacts dicyandiamide with phosphoric acid for 35 to 45 minutes in water to form guanylurea phosphate (GUP), in a solution that contains 50-70 percent solids. The reaction is only allowed to proceed to about 80-95 percent completion, in order to prevent the formation of insoluble precipitates. Boric acid is then mixed with the GUP solution, and the mixture cooled to ambient temperature and diluted to from 3 to 18 percent solids.

Sources & evidence

ORD record
ord-eef2f4d963ce47dea98791d40b4b3675
Source dataset
uspto-grants-2003_11
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US06652633B2

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes