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Adipic Acid → Potassium adipate

HRID 480991
Notes
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Reaction equation

HRID 480991 reaction equation
C(O[K:6])(C)(C)C.[C:7]([OH:16])(=[O:15])[CH2:8][CH2:9][CH2:10][CH2:11][C:12]([OH:14])=[O:13]>CO>[C:7]([O-:16])(=[O:15])[CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O-:14])=[O:13].[K+:6].[K+:6]
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 196Adipic AcidHCID 178418922HCID 178418922, compound

Product 1

HCID 9794493Potassium adipate

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

tert-Butoxypotassium (7.68 g, 68.4 mmol) was dissolved in methanol (100 mL) and then adipic acid (5.0 g, 34.2 mmol) was added to the solution. After stirring the reaction mixture at room temperature for a while, the mixture was concentrated and the residue dried to give dipotassium adipate.

Workup

  1. concentrationthe mixture was concentrated
  2. customthe residue dried

Sources & evidence

ORD record
ord-706a509aa4aa451db439bf60c8e51bc2
Source dataset
uspto-grants-2003_11
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US06653429B1

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes