Methyl chloroformate → 4-(1,1-Dimethyl-3-methoxycarbonyl-2-propynyl)anisole

HRID 481528

Reaction equation

HRID 481528 reaction equation

[CH3:1][C:2]([C:8]1[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][CH:9]=1)([CH3:7])[CH:3]=[C:4](Br)Br.Cl[C:17]([O:19][CH3:20])=[O:18].CC(C1C=CC(OC)=CC=1)(C)C#CC>>[CH3:1][C:2]([C:8]1[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][CH:9]=1)([CH3:7])[C:3]#[C:4][C:17]([O:19][CH3:20])=[O:18]

Participants

4

Reactant 3

HCID 6586Methyl chloroformate

HCID 190664224-(1,1-Dimethyl-3,3-dibromo-2-propenyl)anisole

HCID 190665084-(1,1-Dimethyl-2-butynyl)anisole

Product 1

HCID 190664464-(1,1-Dimethyl-3-methoxycarbonyl-2-propynyl)anisole

Procedure

This compound was prepared from Compound 53 and ClCO2Me in the same manner of Compound 54.

Sources & evidence

ORD record: ord-474fdd2d55754dd0ab9f493f66a4636c
Source dataset: uspto-grants-1998_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05789423

Linked notes

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