2-Hexyl-1-decanol → 4-Phenylpyrimidine-5-carboxylic acid

HRID 482850

Reaction equation

HRID 482850 reaction equation
C(C(CCCCCCCC)CO)CCCCC.[C:18]1([C:24]2[C:29]([C:30]([O:32]CC)=[O:31])=[CH:28][N:27]=[CH:26][N:25]=2)[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>[Hg]>[C:18]1([C:24]2[C:29]([C:30]([OH:32])=[O:31])=[CH:28][N:27]=[CH:26][N:25]=2)[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1

Participants

4

Reactant 2

HCID 953372-Hexyl-1-decanolHCID 23326135HCID 23326135, compound

Product 1

HCID 221623994-Phenylpyrimidine-5-carboxylic acid

Reagents, catalysts & solvents 1

HCID 23931MercuryCatalyst

Procedure

The 2-hexyldecyl ester of 4-phenylpyrimidine-5-carboxylic acid was prepared from 2-hexyldecanol and 4-phenyl-5-ethoxycarbonylpyrimidine using the general procedure of Example 7. The product had a boiling range of 206°-208° C. at 0.2 mm pressure of mercury.

Sources & evidence

ORD record
ord-273d159fe70d4b43898426195d730e0f
Source dataset
uspto-grants-1986_03
Patent number
US04576815

Linked notes

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