HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → 2-[2-(Diethylamino)ethyl]-2,3-dihydro-4-methylpyrido[3,2-f][1,4]oxazepine-5(4H)-thione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 2-(chloroethyl)-2,3-dihydro-4-methylpyrido[3,2-f]-1,4-oxazepine-5(4H)thione | HCID 13726442 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-[2-(Diethylamino)ethyl]-2,3-dihydro-4-methylpyrido[3,2-f][1,4]oxazepine-5(4H)-thione | HCID 13726502 | — |
Reaction Steps
2-(2-Chloroethyl)-2,3-dihydro-4-methylpyrido[3,2-f][1,4]-oxazepine-5(4H)-thione and diethylamine in ethanol are heated together to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04727152 |
| Source dataset | uspto-grants-1988_02 |
| ORD ID | ord-020326b1e4574d44986493bf5d683e46 |
| Source note | uspto-grants-1988_02 |