Thionyl Chloride → 2-(Octyloxy)benzoyl chloride

Reaction equation

[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12](O)=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:21])=O>>[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12]([Cl:21])=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

Reactant 2

HCID 24386Thionyl Chloride

HCID 200827752-(Octyloxy)benzoic acid

Product 1

HCID 203111572-(Octyloxy)benzoyl chloride

Procedure

First, octyloxybenzoic acid was heated in thionyl chloride under reflux until complete dissolution. Excess thionyl chloride was removed by vacuum distillation. Thus there was obtained octyloxybenzoic acid chloride.

Workup

temperatureunder reflux until complete dissolution
customExcess thionyl chloride was removed by vacuum distillation

Sources & evidence

ORD record: ord-65b436956dee4667b9a4e64adcfcd867
Source dataset: uspto-grants-1993_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05225105

Reaction notes

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