2-Methyl-4-nitroaniline → HCID 131714295, compound

Reaction equation

[Cl:1][C:2]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][N:3]=1.[CH3:9][C:10]1[CH:16]=[C:15]([N+:17]([O-])=O)[CH:14]=[CH:13][C:11]=1[NH2:12]>>[ClH:1].[ClH:1].[CH3:9][C:10]1[CH:16]=[C:15]([NH2:17])[CH:14]=[CH:13][C:11]=1[NH:12][C:2]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][N:3]=1

Participants

Reactant 2

HCID 74412-Methyl-4-nitroaniline

HCID 124293887-Chloro-3,4,5,6-tetrahydro-2H-azepine

Product 1

HCID 131714295HCID 131714295, compound

Procedure

The title compound was prepared by the methods of Examples 8 and 9 using 2-chloroazacyclohept-1-ene (0.2 mole), prepared as in Example 3, and 15.2 g (0.1 mole) of 2-methyl-4-nitroaniline. Structure assignment was supported by elemental analysis.

Sources & evidence

ORD record: ord-4b0cff8793494b1d8f3332c18b163bf2
Source dataset: uspto-grants-1985_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04533739

Reaction notes

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