2-Methyl-3-nitroaniline → HCID 69930068, compound

HRID 484807

Reaction equation

HRID 484807 reaction equation
[Cl:1][C:2]1[CH2:6][CH2:5][CH2:4][N:3]=1.[CH3:7][C:8]1[C:14]([N+:15]([O-])=O)=[CH:13][CH:12]=[CH:11][C:9]=1[NH2:10]>>[ClH:1].[ClH:1].[CH3:7][C:8]1[C:9]([NH2:10])=[CH:11][CH:12]=[CH:13][C:14]=1[NH:15][C:2]1[CH2:6][CH2:5][CH2:4][N:3]=1

Participants

3

Reactant 2

HCID 117832-Methyl-3-nitroanilineHCID 135201412-Chloro-1-pyrroline

Product 1

HCID 69930068HCID 69930068, compound

Procedure

The title compound (20.9 g) was prepared by the methods of Examples 8 and 9 using 2-chloro-1-pyrroline, prepared as in Example 1, and 30.0 g of 2-methyl-3-nitroaniline. Structure assignment was supported by the nmr spectrum and by elemental analysis.

Sources & evidence

ORD record
ord-295562804b2b4a26953fd879ae21187d
Source dataset
uspto-grants-1985_08
Patent number
US04533739

Linked notes

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