Ammonia → 4-Amino-1,2,2,6,6-pentamethylpiperidine

HRID 484940

Reaction equation

[CH3:1][N:2]1[C:7]([CH3:9])([CH3:8])[CH2:6][C:5](=O)[CH2:4][C:3]1([CH3:12])[CH3:11].[NH3:13]>>[NH2:13][CH:5]1[CH2:6][C:7]([CH3:9])([CH3:8])[N:2]([CH3:1])[C:3]([CH3:12])([CH3:11])[CH2:4]1

Participants

Reactant 2

HCID 222Ammonia

HCID 2419551,2,2,6,6-Pentamethyl-4-piperidone

Product 1

HCID 6937924-Amino-1,2,2,6,6-pentamethylpiperidine

Procedure

The procedure described in Preparation 1(a) was repeated, but using as starting materials 1,2,2,6,6-pentamethyl-4-piperidone and ammonia, to give the title compound, boiling at 76°-79.5° C./5 mmHg (667 Pascals).

Sources & evidence

ORD record: ord-0bb84f39270b47eb9ff8b0b79444b8a9
Source dataset: uspto-grants-1985_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04533688

Linked notes

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