Phosgene → N-(3-methylphenyl)-N-phenylcarbamoyl chloride
Reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([NH:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:3]=1.[C:15](Cl)([Cl:17])=[O:16]>C1(C)C=CC=CC=1>[CH3:1][C:2]1[CH:3]=[C:4]([N:8]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[C:15]([Cl:17])=[O:16])[CH:5]=[CH:6][CH:7]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
According to the procedure of Example 15, Step A, 3.66 g (20 mmole) of 3-methyldiphenylamine, 20 mL (38.6 mmole) of 1.93M phosgene is toluene solution, and 20 mL of toluene gave 4.9 g (100%) of a dark solid.
Sources & evidence
- ORD record
- ord-c8b6ad109a0f474492295ae76f851cda
- Source dataset
- uspto-grants-1994_03
- Patent number
- US05292726
Reaction notes
Loading…