Phenylacetylene → HCID 9880233, compound

Reaction equation

Br[C:2]1[N:3]([CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[C:4]([Cl:8])=[C:5]([Cl:7])[N:6]=1.[C:15]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)#[CH:16]>>[CH2:13]([O:12][C:10](=[O:11])[CH2:9][N:3]1[C:4]([Cl:8])=[C:5]([Cl:7])[N:6]=[C:2]1[C:16]#[C:15][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[CH3:14]

Participants

Reactant 2

HCID 10821Phenylacetylene

HCID 2778892ethyl 2-(2-bromo-4,5-dichloro-1H-imidazol-1-yl)acetate

Product 1

HCID 9880233HCID 9880233, compound

Procedure

The title compound, MS: m/e=323.0 (M+H+) was prepared in accordance with the general method of example 1b from ethyl (2-bromo-4,5-dichloroimidazole-1-yl)acetate and ethynylbenzene.

Sources & evidence

ORD record: ord-60bd03612aa64ae19383139d5c2cef03
Source dataset: uspto-grants-2005_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06972299B2

Reaction notes

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