Methanol → Methyl 2,6-dihydroxy-4-methoxybenzoate

HRID 488674

Reaction equation

[OH:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]([OH:11])[C:3]=1[C:4]([O-:6])=[O:5].[OH:12][CH2:13]CCCNC(=O)OC(C)(C)C.[CH3:25]O>>[OH:1][C:2]1[CH:10]=[C:9]([O:12][CH3:13])[CH:8]=[C:7]([OH:11])[C:3]=1[C:4]([O:6][CH3:25])=[O:5]

Participants

Reactant 3

HCID 887Methanol

HCID 545141tert-Butyl N-(4-hydroxybutyl)carbamate

HCID 178524827HCID 178524827, compound

Product 1

HCID 264369Methyl 2,6-dihydroxy-4-methoxybenzoate

Procedure

The tilted compound was prepared according to the procedure described for Example 12A, substituting 2,4,6-trihydroxybenzoate for 2,6-dihydroxybenzoate and methanol for tert-butyl 4-hydroxybutylcarbamate.

Workup

customThe tilted compound was prepared

Sources & evidence

ORD record: ord-464a30dcff8d4624962a9c6d997ffe0c
Source dataset: uspto-grants-2005_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06972340B2

Linked notes

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