HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Methyl 3-(bromomethyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Benzoic acid, 3-methyl-, methyl ester | HCID 7435 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Product | Methyl 3-(bromomethyl)benzoate | HCID 517981 | — |
Reaction Steps
Methyl m-toluate was brominated with NBS and AIBN as described in Example 21 to give methyl m-bromomethylbenzoate, and this was further reacted with triethyl phosphite as described in Example 2 without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05242908 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-72cd4b260c0043e8aa2503a92dce1f5e |
| Source note | uspto-grants-1993_09 |