HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Ethyl o-bromomethylphenylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | o-Tolylacetic acid | HCID 69519 | — |
| Product | Ethyl o-bromomethylphenylacetate | HCID 13052926 | — |
Reaction Steps
o-Tolylacetic acid was brominated with NBS and AIBN as described in Example 21 to give ethyl o-bromomethylphenylacetate, and this was reacted with triethyl phosphite as described in Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05242908 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-67807ba4f6aa49a6bfa5666d55bc49c7 |
| Source note | uspto-grants-1993_09 |