Reaction equation
[CH2:1]([C:6]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)([CH2:11][CH2:12][CH:13]([CH3:15])[CH3:14])[C:7]([O:9]C)=[O:8])[CH2:2][CH:3]([CH3:5])[CH3:4].C1(C(CCC)(CCC)C(OC)=O)C=CC=CC=1>>[CH2:1]([C:6]([C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1)([CH2:11][CH2:12][CH:13]([CH3:14])[CH3:15])[C:7]([OH:9])=[O:8])[CH2:2][CH:3]([CH3:5])[CH3:4]Participants
3
Procedure
The title compound was prepared following the procedure of Example 1C, substituting the product of Example 6B for the product of Example 1B. 1H NMR (300 MHz, CDCl3): δ 7.28 (m, 5 H), 2.01 (m, 4 H), 1.49 (m, 2 H), 0.98 (m, 4 H), 0.87 (m, 12 H).
Sources & evidence
- ORD record
- ord-ad1cd0b6d90d4be5aad85ec11efe1b3e
- Source dataset
- uspto-grants-2009_05
- Patent number
- US07538105B2
Linked notes
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