3-Chloro-1-butene → N-{2-[(1-Methyl-2-propenyl)oxy]phenyl}acetamide

HRID 496221

Reaction equation

HRID 496221 reaction equation
Cl[CH:2]([CH3:5])[CH:3]=[CH2:4].[C:6]([NH:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[OH:16])(=[O:8])[CH3:7]>>[CH3:5][CH:2]([O:16][C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=1[NH:9][C:6](=[O:8])[CH3:7])[CH:3]=[CH2:4]

Participants

3

Reactant 2

HCID 112423-Chloro-1-buteneHCID 119722-Acetamidophenol

Product 1

HCID 22313621N-{2-[(1-Methyl-2-propenyl)oxy]phenyl}acetamideYield 40.2%

Procedure

The compound (557 mg, 40%) was prepared from 3-chloro-1-butene (747 ml, 7.42 mmol) and 2-acetamidophenol (1.02 g, 6.75 mmol) analogously to that described in Example 8 i).

Sources & evidence

ORD record
ord-44a90c2b2ca94b97ac759a4b9ca911e6
Source dataset
uspto-grants-2005_09
Patent number
US06943188B2

Linked notes

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