HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → Dicyclopentadiene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Cyclopentadiene | HCID 7612 | — |
| Reactant | Acrylate | HCID 25188 | — |
| Product | Dicyclopentadiene | HCID 6492 | — |
Reaction Steps
The derivative was synthesized as follows. 20 grams of the derivative of acrylate obtained as the third example was dissolved in 20 milliliters of toluene. 7 grams of cyclopentadiene was dropped into the solution cooled with ice, and was agitated through all night. Dicyclopentadiene was produced as by-product, and was eliminated in vacuum. Then, 24.9 grams of the derivative of norbornene was obtained. The derivative of norbornene was viscous liquid, and the yield was 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06710188B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-ed221a40b0554bbd900e864b34ebf7eb |
| Source note | uspto-grants-2004_03 |