4-Methyl-1-pentanol → HCID 22736017, compound

HRID 50977

Reaction equation

[CH3:1][CH:2]([CH3:7])[CH2:3][CH2:4][CH2:5][OH:6].[CH3:8][S:9](Cl)(=[O:11])=[O:10]>>[CH3:8][S:9]([O:6][CH2:5][CH2:4][CH2:3][CH:2]([CH3:7])[CH3:1])(=[O:11])=[O:10]

Participants

Reactant 2

HCID 122964-Methyl-1-pentanol

HCID 31297Methanesulfonyl chloride

Product 1

HCID 22736017HCID 22736017, compound

Procedure

The title compound was prepared by following the general procedure of Example 43 for mesylation as a colorless oil (620 mg, 63%) from 4-methyl-1-pentanol (511 mg, 5.00 mmol) and methanesulfonyl chloride (844 mg, 7.50 mmol). 1H NMR (CDCl3, 300 MHz) δ0.88 (d, 6H, J=4.7 Hz), 1.23-1.31 (m, 2H), 1.53-1.62 (m, 1H), 1.70-1.80 (m, 2H), 3.00 (s, 3H), 4.21 (t, 2H, J=6.6 Hz) ppm.

Sources & evidence

ORD record: ord-eb37cb96c3ac4a40b1d317c93abe9152
Source dataset: uspto-grants-2004_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06713471B1

Linked notes

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