Prolinol, (R)- → HCID 59547752, compound

Reaction equation

[CH2:1]([S:4]([O:7][CH2:8][CH2:9][N:10]([CH3:17])[S:11]([CH2:14][CH2:15][CH3:16])(=[O:13])=[O:12])(=[O:6])=[O:5])[CH2:2][CH3:3].N1CC[CH2:20][C@@H:19]1CO>>[CH2:14]([S:11]([N:10]1[CH2:17][CH2:20][CH2:19][C@@H:9]1[CH2:8][O:7][S:4]([CH2:1][CH2:2][CH3:3])(=[O:6])=[O:5])(=[O:13])=[O:12])[CH2:15][CH3:16]

Participants

Reactant 2

HCID 2724541Prolinol, (R)-

HCID 57471221HCID 57471221, compound

Product 1

HCID 59547752HCID 59547752, compound

Procedure

Prepared as described for 2-(N-methylpropylsulfonamido)ethyl propane-1-sulfonate (example 76, step 1 using (R)-1-pyrrolidin-2-yl-methanol instead of 2-(methylamino)ethanol.

Workup

customPrepared

Sources & evidence

ORD record: ord-7165a5e79275415d9ed0496a7aaf2849
Source dataset: uspto-grants-2015_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09096619B2

Reaction notes

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