HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiophenecarboxaldehyde → HCID 178524223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiophenecarboxaldehyde | HCID 7364 | — |
| Reactant | Benzoyl chloride, 3,4-dichloro- | HCID 76403 | — |
| Reactant | Fmoc-leucine | HCID 1549133 | — |
| Reactant | HCID 178523876 | HCID 178523876 | — |
| Product | HCID 178524223 | HCID 178524223 | — |
Reaction Steps
Following the procedure of Example 28(a)-28(d), except beginning with Wang bound Fmoc-L-histidine (Trt) instead of Wang bound Fmoc-L-leucine, and substituting furan-2-carboxaldehyde for thiophene-2-carboxaldehyde, and substituting 4-chlorobenzoylchloride for 3,4-dichlorobenzoyl chloride, the title compound was prepared as a solid. MS [M+H]+444.8
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06713502B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-3adcf0f3a9694e53b5a862322e9894d9 |
| Source note | uspto-grants-2004_03 |