Reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[CH:10]=[CH:9][N:8]=[C:7]([O:11][CH2:12]/[CH:13]=[CH:14]\[CH2:15][NH2:16])[CH:6]=1)[CH3:3].[O:17]1[CH2:22][CH2:21][S:20][CH2:19][C:18]1=[O:23]>>[CH3:1][N:2]([CH2:4][C:5]1[CH:10]=[CH:9][N:8]=[C:7]([O:11][CH2:12]/[CH:13]=[CH:14]\[CH2:15][NH:16][C:18](=[O:23])[CH2:19][S:20][CH2:21][CH2:22][OH:17])[CH:6]=1)[CH3:3]Participants
3
Procedure
Following a procedure similar to that described in Example 68, but using 4-(4-dimethylaminomethyl-2-pyridyloxy)-cis-2-butenylamine and 1,4-oxathian-2-one as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained in a 53% yield.
Sources & evidence
- ORD record
- ord-f37fbe5f088f4ce5998302782341a4c9
- Source dataset
- uspto-grants-1997_04
- Patent number
- US05616579
Linked notes
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