N-(tert-Butoxycarbonyl)-N'-methylethylenediamine → HCID 67121289, compound

HRID 527391

Reaction equation

HRID 527391 reaction equation
C([O:3][C:4]([CH2:6][S:7][C:8]1[CH:16]=[CH:15][C:11]([C:12]([OH:14])=O)=[CH:10][CH:9]=1)=[O:5])C.[C:17]([O:21][C:22](=[O:28])[NH:23][CH2:24][CH2:25][NH:26][CH3:27])([CH3:20])([CH3:19])[CH3:18]>>[C:17]([O:21][C:22]([NH:23][CH2:24][CH2:25][N:26]([CH3:27])[C:12]([C:11]1[CH:10]=[CH:9][C:8]([S:7][CH2:6][C:4]([OH:3])=[O:5])=[CH:16][CH:15]=1)=[O:14])=[O:28])([CH3:20])([CH3:19])[CH3:18]

Participants

3

Reactant 2

HCID 3435744N-(tert-Butoxycarbonyl)-N'-methylethylenediamineHCID 43352345HCID 43352345, compound

Product 1

HCID 67121289HCID 67121289, compound

Procedure

{4-[(2-Tert-butoxycarbonylaminoethyl)methylcarbamoyl]phenylthio}acetic acid was prepared in analogy to the procedure described in example 80 using 4-ethoxycarbonylmethylsulfanylbenzoic acid and commercially available (2-methylamino-ethyl)carbamic acid tert-butyl ester.

Sources & evidence

ORD record
ord-e0e7efb838724b37869597120a3f6ba7
Source dataset
uspto-grants-2016_05
Patent number
US09346799B2

Linked notes

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