HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → Formamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | Methyl 3-carbamoylisobutyrate | HCID 11768702 | — |
| Product | Formamide | HCID 713 | — |
| Product | Methylsuccinic acid ethyl methyl ester | HCID 54001611 | — |
Reaction Steps
The procedure in Example 3 (3) was repeated except that ethyl formate was used in place of methyl formate. As a result, the conversion of methyl 3-carbamoylisobutyrate was 83.7% and there were obtained methylsuccinic acid ethyl methyl ester at a selectivity of 99.8% and formamide at a selectivity of 98.6%, each based on the reacted methyl 3-carbamoylisobutyrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05618953 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-0b2414389f2d435ebd782a575159d2a6 |
| Source note | uspto-grants-1997_04 |