HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → N-Cyclohexylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Nitrobenzene | HCID 7416 | — |
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | Diphenylamine | HCID 11487 | — |
| Reactant | Triphenylamine | HCID 11775 | — |
| Product | N-Cyclohexylaniline | HCID 74567 | 2.9% |
Reaction Steps
Reaction was carried out by the same procedure as in Example I1 except that 32.39 g (0.39 mol) of cyclohexanone, 9.31 g (0.1 mol) of aniline and 24.62 g (0.2 mol) nitrobenzene were used. As a result, the yield of diphenylamine was 89.5%, and 1.8% of triphenylamine and 2.9% of N-cyclohexylaniline were produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05618980 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-6a4a9d71f6204543b7bc12d011dc8c18 |
| Source note | uspto-grants-1997_04 |