1-Naphthylamine → Ethyl N-naphthalen-1-ylpropionimidate

Reaction equation

[NH2:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1.[CH2:12]([O:14][C:15](OCC)(OCC)[CH2:16][CH3:17])[CH3:13]>>[C:2]1([N:1]=[C:15]([O:14][CH2:12][CH3:13])[CH2:16][CH3:17])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 86401-Naphthylamine

HCID 66995Ethyl orthopropionate

Product 1

HCID 66852489Ethyl N-naphthalen-1-ylpropionimidate

Procedure

The title compound was prepared from 1-aminonaphthalene and triethylorthopropionate according to the following procedure: DeWolfe, R. H. J. Org. Chem. 1962, 27, 490-493.

Sources & evidence

ORD record: ord-d9c74bc5bdd7441b88d976976834e220
Source dataset: uspto-grants-2014_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08865753B2

Reaction notes

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