HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ferulic Acid → Dihydroferulic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ferulic Acid | HCID 445858 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Dihydroferulic Acid | HCID 14340 | 95.5% |
Reaction Steps
20.0 g of Ferulic acid was dissolved in 250 ml of methanol and subjected to catalytic reduction under normal pressure for 3 hours in the presence of 10% palladium carbon catalyst (50% wet type). After removing the catalyst by filtration, the resulting filtrate was concentrated to collect precipitated crystals by filtration, thereby obtaining 19.3 g of 3-(4-hydroxy-3-methoxyphenyl)propionic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05620991 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-82b17ac5b1d24f1eb4c9fd8d2d950180 |
| Source note | uspto-grants-1997_04 |