2',4'-Dihydroxyacetophenone → Ethyl hexanoate

HRID 543217

Reaction equation

HRID 543217 reaction equation
C(C1C=CC([CH:14](Br)[CH2:15][CH2:16][CH2:17][CH2:18][C:19]([O:21][CH2:22][CH3:23])=[O:20])=CC=1)C1C=CC=CC=1.CC(C1C=CC(O)=CC=1O)=O>>[C:19]([O:21][CH2:22][CH3:23])(=[O:20])[CH2:18][CH2:17][CH2:16][CH2:15][CH3:14]

Participants

3

Reactant 2

HCID 69902',4'-DihydroxyacetophenoneHCID 13881964HCID 13881964, compound

Product 1

HCID 31265Ethyl hexanoate

Procedure

Following the procedure of Example 15, 3.75 g. of ethyl 6-(4-benzylphenyl)-6-bromo-hexanoate and 1.94 g. of 2,4-dihydroxyacetophenone were reacted to provide the intermediate ethyl hexanoate derivative which was then hydrolyzed to provide 0.95 g. of the title product as an oil.

Sources & evidence

ORD record
ord-75e0d54fe36542b586511d33af2d95ca
Source dataset
uspto-grants-1987_04
Patent number
US04661505

Linked notes

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