2-Propenoic acid, 3-hydroxypropyl ester → Isopropenylphosphonic Acid Hydroxypropylacrylate

HRID 543455

Reaction equation

HRID 543455 reaction equation
[C:1]([P:4](=[O:7])([OH:6])[OH:5])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]>O>[C:1]([P:4](=[O:5])([OH:7])[OH:6])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]

Participants

4

Reactant 2

HCID 331012-Propenoic acid, 3-hydroxypropyl esterHCID 557541Isopropenylphosphonic acid

Product 1

HCID 86739384Isopropenylphosphonic Acid Hydroxypropylacrylate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Used the method of Example 5, isopropenyl phosphonic acid (30.7 g, 54%, 0.14 mole), hydroxypropylacrylate (36.4 g, 0.28 mole) and water (144.9 g) were charged in the reactor. The bulk of the polymer crystallized during the first period of reflux and was found to be insoluble in water.

Workup

  1. customThe bulk of the polymer crystallized during the first period
  2. temperatureof reflux

Sources & evidence

ORD record
ord-49e0e65a7ace49c29f56fbb104f02e73
Source dataset
uspto-grants-1984_05
Patent number
US04446028

Linked notes

Loading…