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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 545231Generated: October 23, 2026

Benzene, 1-fluoro-2-methyl-4-nitro- → HCID 61151226, compound

https://huagongshe.com/en/reaction/545231

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzene, 1-fluoro-2-methyl-4-nitro-HCID 68001—
ReactantDiisopropylethylamineHCID 81531—
Reactant1-(2-Ethoxyethyl)piperazineHCID 2734643—
SolventDimethyl SulfoxideHCID 679—
ProductHCID 61151226HCID 61151226—

Reaction Steps

In the same manner as in Production Example 5-1, but using 4-(2-ethoxyethyl)piperazine in place of N-ethylpiperazine used in Production Example 5-1, using 5-nitro-2-fluorotoluene in place of 2-fluoro-5-nitrobenzyl alcohol, using N,N-diisopropylethylamine in place of potassium carbonate, and using dimethylsulfoxide in place of N-methylpyrrolidone, the entitled compound was obtained as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07935708B2
Source datasetuspto-grants-2011_05
ORD IDord-1118415f06c340358225aa91bac29e97
Source noteuspto-grants-2011_05