3,4-Difluorophenol → HCID 178461114, compound

HRID 54881

Reaction equation

HRID 54881 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[CH:6][C:7]=1[F:8].C1([Si:16]2([CH2:31][CH2:32][CH2:33][CH:34]([F:36])[CH3:35])[CH2:21][CH2:20][CH:19]([C:22]3[CH:30]=[CH:29][C:25]([C:26](O)=[O:27])=[CH:24][CH:23]=3)[CH2:18][CH2:17]2)C=CC=CC=1>>[F:36][CH:34]([CH3:35])[CH2:33][CH2:32][CH2:31][Si@H:16]1[CH2:21][CH2:20][C@H:19]([C:22]2[CH:23]=[CH:24][C:25]([C:26]([O:9][C:4]3[CH:5]=[CH:6][C:7]([F:8])=[C:2]([F:1])[CH:3]=3)=[O:27])=[CH:29][CH:30]=2)[CH2:18][CH2:17]1

Participants

3

Reactant 2

HCID 759273,4-DifluorophenolHCID 199567624-(4-Phenyl-4-(4-fluoropentyl)-4-silacyclohexyl)benzoic acid

Product 1

HCID 178461114HCID 178461114, compound

Procedure

The general procedure of Example 3 was repeated using 3,4-difluorophenol and 4-(4-phenyl-4-(4-fluoropentyl)-4-silacyclohexyl)benzoic acid, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-01405a98801a4eaebd13b07ad94afb1b
Source dataset
uspto-grants-1997_04
Patent number
US05624601

Linked notes

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