Benzeneacetic acid, hydrazide → HCID 57691923, compound

HRID 550539Notes

Reaction equation

HRID 550539 reaction equation
[C:1]1([CH2:7][C:8]([NH:10][NH2:11])=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[CH3:13][NH:14][C:15](=NC)[CH2:16][CH2:17][CH2:18][CH:19]=[CH2:20]>>[CH3:13][N:14]1[C:8]([CH2:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)=[N:10][N:11]=[C:15]1[CH2:16][CH2:17][CH2:18][CH:19]=[CH2:20]

Participants

3

Reactant 2

HCID 70301Benzeneacetic acid, hydrazideHCID 86630240N,N'-dimethyl-5-hexenimidamide hydrochloride

Product 1

HCID 57691923HCID 57691923, compound

Procedure

The title compound was prepared in analogy to Preparation 11 in 0.18 g yield starting from phenylacetic hydrazide (0.5 g) and N,N′-dimethyl-5-hexenimidamide hydrochloride (0.62 g). MS (m/z): 242 [MH]+.

Workup

  1. customyield

Sources & evidence

ORD record
ord-f45196db51994916a0dd8b2296c4e87a
Source dataset
uspto-grants-2011_05
Patent number
US07947683B2

Reaction notes

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