Aluminium lithium hydride → HCID 55285947, compound

Reaction equation

[CH3:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][N+:9]([O-])=O)[S:5][CH:6]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH3:1][C:2]1[CH:3]=[C:4]([CH2:7][CH2:8][NH2:9])[S:5][CH:6]=1

Participants

Reactant 2

HCID 21226445Aluminium lithium hydride

HCID 67192637HCID 67192637, compound

Product 1

HCID 55285947HCID 55285947, compoundYield 85%

Procedure

In close analogy to the procedure described above, 4-Methyl-2-(2-nitro-vinyl)-thiophene is reacted with lithium aluminium hydride to provide the title compound.

Sources & evidence

ORD record: ord-3193b387fde14524a72b51bc69b56d39
Source dataset: uspto-grants-2011_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07947689B2

Reaction notes

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