Phosphorus oxide (P4O10) → HCID 59663081, compound

Reaction equation

[CH3:1][C:2]1[CH:3]=[C:4]([CH2:7][CH2:8][NH:9][C:10](=O)[CH3:11])[S:5][CH:6]=1.O=P12OP3(OP(OP(O3)(O1)=O)(=O)O2)=O>>[CH3:1][C:2]1[C:3]2[C:10]([CH3:11])=[N:9][CH2:8][CH2:7][C:4]=2[S:5][CH:6]=1

Participants

Reactant 2

HCID 14812Phosphorus oxide (P4O10)

HCID 59663085HCID 59663085, compound

Product 1

HCID 59663081HCID 59663081, compound

Procedure

In close analogy to the procedure described above, N-[2-(4-Methyl-thiophen-2-yl)-ethyl]-acetamide is reacted with phosphorus pentoxide to provide the title compound.

Sources & evidence

ORD record: ord-4e5d1330858b44fe8a5e8681b0e0bc64
Source dataset: uspto-grants-2011_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07947689B2

Reaction notes

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