3-Methylhex-5-en-2-one → Methyl 3,4-dimethyl-3-hydroxy-6-heptenoate

HRID 551677

Reaction equation

HRID 551677 reaction equation
[CH2:1]([CH:4]([CH2:12][CH2:13][CH2:14]C)[CH:5]([OH:11])[CH2:6][C:7]([O:9][CH3:10])=[O:8])C=C.[CH3:16]C(CC=C)C(=O)C>>[OH:11][C:5]([CH3:16])([CH:4]([CH3:1])[CH2:12][CH:13]=[CH2:14])[CH2:6][C:7]([O:9][CH3:10])=[O:8]

Participants

3

Procedure

The compound of interest (11.7 g, 60%) was obtained as an oil substance (diastereomeric mixture) in the same way as in paragraph (10-a) using 3-methyl-5-hexen-2-one (17 g, 106 mmol).

Sources & evidence

ORD record
ord-9233128fdd294af09c0d91b43d1ba73a
Source dataset
uspto-grants-2011_05
Patent number
US07947738B2

Linked notes

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