N-bromobutanimide → HCID 66924684, compound
Reaction equation
[CH:1]([C:4]1[C:5]([C:9]([O:11][CH3:12])=[O:10])=[CH:6][NH:7][CH:8]=1)([CH3:3])[CH3:2].[Br:13]N1C(=O)CCC1=O>N1C=CC=CC=1>[Br:13][C:8]1[NH:7][CH:6]=[C:5]([C:9]([O:11][CH3:12])=[O:10])[C:4]=1[CH:1]([CH3:3])[CH3:2]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Using methyl 4-isopropyl-1H-pyrrole-3-carboxylate (3.5 g), N-bromosuccinimide (3.74 g) and pyridine (0.5 mL), a procedure as in Reference Example 40 was performed to give the title compound as colorless crystals (yield 3.29 g, 64%).
Sources & evidence
- ORD record
- ord-1066d0002c7644b4aaccbaeaabaf2a9e
- Source dataset
- uspto-grants-2011_11
- Patent number
- US08048909B2
Reaction notes
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