Dimethyl Disulfide → 2-Methoxy-6-methylsulfanyl-4-trifluoromethyl-benzoic acid

HRID 560195

Reaction equation

[CH3:1][O:2][C:3]1[CH:11]=[C:10]([C:12]([F:15])([F:14])[F:13])[CH:9]=[CH:8][C:4]=1[C:5]([OH:7])=[O:6].[CH3:16][S:17]SC>>[CH3:1][O:2][C:3]1[CH:11]=[C:10]([C:12]([F:13])([F:14])[F:15])[CH:9]=[C:8]([S:17][CH3:16])[C:4]=1[C:5]([OH:7])=[O:6]

Participants

Reactant 2

HCID 12232Dimethyl Disulfide

HCID 36908732-Methoxy-4-(trifluoromethyl)benzoic acid

Product 1

HCID 591979212-Methoxy-6-methylsulfanyl-4-trifluoromethyl-benzoic acid

Procedure

The title compound, white solid, MS: m/e=265.1 [(M−H)−], was prepared in accordance with the general method of intermediate E from 2-methoxy-4-(trifluoromethyl)benzoic acid and dimethyl disulfide.

Sources & evidence

ORD record: ord-838376c5327143fe8655b751d4bfcc12
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08063098B2

Linked notes

Loading…