Tolylboronic acid → 2-Thiophenecarboxylic acid, 3-(4-methylphenyl)-
Reaction equation
Br[C:2]1[CH:6]=[CH:5][S:4][C:3]=1[C:7]([OH:9])=[O:8].B(O)(O)[C:11]1[CH:12]=[CH:13][C:14]([CH3:17])=[CH:15][CH:16]=1>>[C:14]1([CH3:17])[CH:15]=[CH:16][C:11]([C:2]2[CH:6]=[CH:5][S:4][C:3]=2[C:7]([OH:9])=[O:8])=[CH:12][CH:13]=1Participants
3
Procedure
prepared by reaction of 3-bromo-thiophene-2-carboxylic acid with p-tolylboronic acid. LC-MS (basic): tR=0.50 min; [M−H]−=217.2.
Sources & evidence
- ORD record
- ord-8df1640873464e7c947a368084e09cdd
- Source dataset
- uspto-grants-2011_11
- Patent number
- US08063099B2
Reaction notes
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