HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Fluorophenyl)-2-(piperazin-1-yl)ethan-1-one dihydrochloride → HCID 178521227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Fluorophenyl)-2-(piperazin-1-yl)ethan-1-one dihydrochloride | HCID 42933716 | — |
| Reactant | HCID 178524948 | HCID 178524948 | — |
| Product | HCID 178521227 | HCID 178521227 | 65.3% |
Reaction Steps
The title compound was prepared in a similar manner as described in Example 1.2, using 4-chloro-1H-pyrazole-3-carboxylic acid (22.0 mg), and 1-(4-fluorophenyl)-2-(piperazin-1-yl)ethanone dihydrochloride (29.5 mg) as starting materials, to afford the title compound (22.9 mg) as a white solid. Exact mass calculated for C16H16ClFN4O2: 350.1. Found: LCMS m/z (%)=351.3 (M+H+35Cl, 100%), 353.3 (M+H+37Cl, 32%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434692B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-a3055e906fc847649f9027cead46efa8 |
| Source note | uspto-grants-2016_09 |